Test and Calibration Instrumentation

Instrument Calibration must be carried out to maintain and verify instrument accuracy. Test and Calibration instruments are available that cover all different instruments which measure typically Flow, Pressure, Temperature etc. They are also used for setting up final elements such as control valves. Test and Calibration instruments are available in portable versions for site calibration or bench versions for the workshop. Calibration is the process of configuring an instrument to provide a result for a sample within an acceptable range. Eliminating or minimising factors that cause inaccurate measurements is a fundamental aspect of instrumentation design.

There are as many definitions of calibration as there are methods. According to ISA’s The Automation, Systems, and Instrumentation Dictionary, the word calibration is defined as “a test during which known values of measurement are applied to the transducer and corresponding output readings are recorded under specified conditions”. The definition includes the capability to adjust the instrument to zero and to set the desired span. Usually Calibration involves injecting an accurate signal from the calibrator into the instrument at 0%, 25%, 50%, 75% and 100% of range and adjusting the instrument zero and span to a point where the instrument is aligned with the calibrator for the specified range.

Test and Calibration Instrumentation

Thanks to Zedflo Australia for the following information.

Low Pressure Calibrations - When you're performing a low pressure calibration, there are some things you can do to make the job easier and better (more accurate) - From Martel Matters Newsletter.

Temperature Calibrations (Thermocouple Edition) - There are a few "gotchas" in temperature calibration when we're talking about T/Cs and RTDs. Each has its own problems, This article will focus on calibration of T/C instrumentation - From Martel Matters Newsletter.

Field Calibrators Make Everything Better - Users Are Opening Their Eyes to How Much Clearer Their Data Is - and How Much Better Their Processes Can Run - with Field Calibrators - From www.controlglobal.com.

Martel Process Calibrators Blog - Lots of Interesting Calibration Related posts.

Martel Calibrator Newsletter - Martel Matters is an e-newsletter from Martel Calibrators. It provides information on new and existing products and calibration "tips". Highlights from the Latest Newsletter include:

Tips on performing Low Pressure Calibration
Getting Rid Of Leaks
Adding Volume To Your System
Watching Out For Temperature Effects
Considering Head Pressure Errors

“How to” Choose the Right batteries for your Calibrator - Most of our calibrators are designed to use standard replaceable Alkaline batteries. You know, the ones you can buy at the corner store. That’s a good choice because of the relatively high power density and mostly flat discharge curve of these cells. They start out with a high terminal voltage (1.5 V or more). A really strong point for these batteries is the long shelf life. If you don’t use your calibrator much, that would be a good reason to use Alkalines. New ones typically have a shelf life of 3 years or more.

Is It a Calibrator? - People actually in the calibration industry often hear things being called calibrators that obviously aren’t. The defining points for a calibrator are detailed here.

Gas Custody Transfer Calibration - Using Multivariable Temperature / Pressure Calibrators for Flowmeter Calibration - Gas custody transfer flow computers require special calibration to perform at optimum accuracy. In custody transfer applications where the buying and selling of commodities like natural gas is involved, calibration checks are performed frequently as a matter of fiduciary responsibility. For the purpose of this white paper, the use of gas custody transfer flow computers in the natural gas transmission industry is referenced.

Determining Accuracy and Stability for Digital Pressure Gauges - Like all calibration device manufacturers Martel Electronics spends a great deal of time determining what the accuracy specification is for the products we design. General convention is to publish one (1) year specifications as that is the generally accepted calibration interval for most calibration devices. Pressure measuring devices pose interesting challenges when trying to determine the one year specifications because not only must the long term stability of the electrical circuit be determined you must also determine the stability characteristics of the pressure sensor itself over time and combine those two numbers to arrive at a complete specification.

The Calibration of Smart Instrumentation - A Better Way - The assertion often arises that smart instruments don’t need calibration since they are very stable, reliable devices. This assertion ignores certain vital realities. These include: - Field instruments are exposed to harsh environments.

Good practice calls for in situ calibration
Safety Instrumented Systems require periodic calibration
Custody transfer applications require periodic calibration by user demand

What to Look for in a Documenting Calibrator - A documenting calibration system can be as simple as a single multi-function calibrator with an easy to use software package or it can be a more sophisticated system with extensive database software, custom reporting and multiple brands or types of calibrators. There is a lot of choice in the marketplace, so it’s important to determine your needs and buy accordingly rather than having a system that dictates to you.

Martel LC-110H Loop Calibrator and HART Communications/Diagnostics - This white paper describes the basic functions of HART communications and the diagnostic capability of the Martel LC-110H mA (loop) calibrator.

Why Test and Calibration Equipment Is Essential - For the purpose of optimal performance and efficiency, every car needs regular oil changes. This not only helps the engine to run smoothly, it also helps to increase the car’s lifetime. As such, it goes a long in reducing the need to purchase a new car, which is a headache you could do without. Oil change is the same as the calibration. Basically, calibrating a piece of test equipment also ensures that equipment is running efficiently and fine-tuned. This is required for, test equipment to provide accurate test results in the event of default product models. So why is test and calibration equipment in Perth important in the face of advanced technology?

Why Temperature Compensation Really Matters for Pressure Measurement - Jon Sanders - Have you ever wondered how much impact environmental temperature has on your pressure sensors? Nearly every pressure sensor has some sort of environmental temperature specification on its data sheet. This technical note explains the impact of environmental temperature effects on pressure sensors, quantifying the impact and ways to minimize the impact.

The following calibration white papers are from Additel Corporation:

Calibrating Differential Pressure Sensors - How to calibrate a DP sensor and understand some of the calibration challenges associated with them.
Calibrating a Pressure Switch - Pressure switches are commonly used in the process industry for a wide range of applications. A pressure switch is a form of sensor that closes or opens an electrical contact when a certain pressure has been obtained either through a pressure rise or a pressure drop. Pressure switches are used to monitor, control, or provide a caution or warning for a pressure related process. The repeatability, accuracy, and functionality of a pressure switch often tie directly into the safety or efficiency of a process and thus it becomes important that pressure switches are verified and calibrated to ensure their proper function in the process - from Additel Corporation.
Considerations for Hydraulic Pressure Calibrations - Jon Sanders - If you are doing high pressure, hydraulic calibrations there are a few things that you'll need to consider which will make your life a little easier and help you produce stable measurements. This application note focuses on considerations for pressure calibrations using a high pressure hydraulic pump to generate the pressure.
Improved Methods for High Pressure Pneumatic Calibrations in the Field - Jon Sanders - Are you tired of dragging a nitrogen bottle and dead weight tester out to the field to perform pneumatic high pressure calibrations? Does it trouble you to use a hydraulic pump or dead weight tester for your gas gauges every time you have to go above 600 psi? This application note details the limitations to traditional methods and provides a solution to calibration of gas gauges up to 3,000 psi (200 bar) with a field-ready calibration tool.
Understanding Accuracy Specifications for Digital Pressure Sensors - Percentage of Full Scale Versus Percentage of Reading - Jon Sanders - Specifications for digital pressure gauges can sometimes seem confusing or overwhelming, especially, if you are unfamiliar with the terminology. Some pressure sensors will specify accuracy as a percent of full scale (FS) while others provide the specification as a percent of reading. So why are there different ways of specifying the accuracy of pressure sensors and is percent of reading more accurate than percent of full scale or vise versa? This brief technical note will discuss the two differences and answer these questions.

The Following are from the very useful InstrumentationPortal.Com:

Calibration Form - Calibration forms provide a list of actions to be done when performing instrument calibration. Instrument Calibration is required to make sure that instrument will function properly prior to installation. Before shipping, vendor has already done the calibration after setting the range to pre-determined value as requested by the end-user. It is common by contractor to re-check the instrument by performing bench calibration. However, some end-users prefer to install the instrument without undertaking this test. Following are some typical calibration forms for transmitters, gauges and control valves.
Transmitter Calibration Form
Control Valve Calibration Form
Pressure Gauge Calibration Form

Calibration Principles - Details in this excellent ISA document on how to define key terms relating to calibration and interpret the meaning of each. Understand traceability requirements and how they are maintained. It describes the following:

The characteristics of a good control system technician:

Differences between bench calibration and field calibration
The differences between loop calibration and individual instrument calibration, listing the advantages and disadvantages of each.
List the advantages and disadvantages of classifying instruments according to process importance-for example, critical, non-critical, reference only,OSHA,EPA, etc.

Flow and Level Calibration Notes - Thanks to INX Inc - These notes whilst being a little dated are still very useful.

Pressure & Temperature Calibration Notes - Thanks to INX Inc - These notes whilst being a little dated are still very useful.

Calibration Primer - From Omega.com - The most sophisticated industrial equipment will not be very useful unless it is calibrated. Through calibration, adjustments made to a piece of equipment ensure that it performs as expected-that it can be relied on to deliver predictable, accurate results that meet quality standards. This white paper from Omega Engineering explains what calibration is, why it is important, and how it works. NIST traceability is defined and discussed, and there is a step-by-step description of a basic calibration. This paper also discusses in-house vs. laboratory calibration, and it describes major types of calibration devices.

Some Notes on Device Calibration - From the University of Dublin - A comprehensive albeit a bit academic note.

Calibration - Calibration is the validation of specific measurement techniques and equipment. At the simplest level, calibration is a comparison between measurements-one of known magnitude or correctness made or set with one device and another measurement made in as similar a way as possible with a second device. This article from Wikipedia covers all the basics pretty well.

A Beginner’s Guide to Measurement - This 30 page Beginner’s Guide from the National Physical Laboratory explains the fundamental concepts and basic facts about measurement, and in particular accurate measurement. It includes brief accounts of the role of measurement in modern and historical societies and explains the SI system, its base units and their relation to other units. The various organisations involved in measurement are introduced and their roles in linking all measurements to the SI base units through traceability chains explained. It includes general guidance about practical issues that affect the making of measurements, gives the meanings of key measurement terms, and explains the significance of such fundamental concepts as measurement traceability and calibration.

Loop Calibrations - New, More Efficient Methods Improv Productivity - Ned Espy - The typical approach to calibration has been to regularly test instrumentation that affects successful control, safe operation, quality, or other relevant criteria. In most cases, scheduling is conservative, and methods at a particular site have evolved over time. Instrument technicians follow practices that were set up many years ago. It is not uncommon to hear, “this is the way we have always done it”. Measurement technology continues to improve and is getting more accurate. It is also getting more complex-why test a fieldbus transmitter with the same approach as a pneumatic transmitter? Performing the standard five-point, up-down test does not always apply to today’s more sophisticated applications - from the ISA and InTECH.

The Following Technical Tips are from Advanced Instruments Inc:

What Is Instrument Calibration and What Does It Do? - Instrument calibration is one of the primary processes used to maintain instrument accuracy. Calibration is the process of configuring an instrument to provide a result for a sample within an acceptable range. Eliminating or minimizing factors that cause inaccurate measurements is a fundamental aspect of instrumentation design.
Why is Calibration Important? - How a properly performed calibration can improve product performance.
What Factors Affect Calibration? - Once the benefits of a properly performed calibration are understood, it becomes evident that care must be taken during the process to prevent potential error sources from degrading the results. Several factors can occur during and after a calibration that can affect its result.

Calibration Terminology

Calibration Terminology - Details on calibration terms - from Beamex.

The following links are from Fluke:

Calibrating Fieldbus Instruments

Calibrating Fieldbus Transmitters - Fieldbus is becoming more and more common in today’s instrumentation. But what is fieldbus and how does it differ from conventional instrumentation? Fieldbus transmitters must be calibrated as well, but how can it be done? Until now, no practical solutions have existed for calibrating fieldbus transmitters - from Beamex.

Calibration Frequency

Instrument Calibration - Glenn Carlson, Technical Support, - Users frequently want to know how often they need to calibrate their In- Situ instrument. The most accurate answer to that question is “it depends”. This article addresses this - thanks to In-Situ Inc.

How Frequently should a Product be Calibrated? - The simple answer to this question, although not a very helpful one, is “when it needs it”. From a more practical standpoint, daily or periodically testing the control solutions of known values can provide a quantitative indication of instrument performance, which can be used to establish a history - from Advanced Instruments Inc.

How often should Calibrators be Calibrated? - This article discusses some of the things to be considered when specifying the calibration period and provides some general guidelines. The same guidelines that apply to a calibrator also apply to other measuring equipment in the traceability chain. These guidelines can even be used for process instrumentation - from Beamex.

How often should Instruments be Calibrated? - Plants can improve their efficiency and reduce costs by performing calibration history trend analysis. By doing it, a plant is able to define which instruments can be calibrated less frequently and which should be calibrated more frequently. Calibration history trend analysis is only possible with calibration software that provides this functionality - from Beamex.

Calibration Intervals, A Manufacturer’s Perspective - David Deaver - The analysis tools that are currently available for Calibration Intervals focus on setting intervals to achieve a desired reliability target. This paper suggests there is another perspective that these tools do not currently address; consequence cost or accumulated liability. A case is made that sometimes the reliability target is a secondary consideration to managing this consequence cost. The paper also addresses how manufacturers establish calibration intervals. The paper presents, and defends, the practice of using no analysis whatsoever in establishing the manufacturer's recommended calibration interval - from Fluke.

Calibration Advantages using Electronic Device Description Language (EDDL) Technology

The following white papers and articles are from the EDDL group:

Calibration Trim - EDDL technology makes calibration easier thanks to user guidance such as wizards as well as know-how made available from the device manufacturer's experts. The result is lower cost of maintenance, and better performing devices.
Intelligent Device Management Tutorial: Calibration - In the early days of smart transmitters the concept of remote range setting ("remote calibration") and re-ranging without applying input was revolutionary. It took years of education to be accepted and understood. Calibration can be carried out using a handheld communicator in the field, a laptop in the workshop, or from intelligent device management software as part of an asset management solution. Electronic Device Description Language (EDDL) is the technology used by device manufacturers to define how the system shall display the device information and functions to the technician. EDDL makes calibration of smart transmitters and other intelligent devices easier thanks to user guidance such as wizards and help, and unparalleled consistency of use.
EDDL Solution for Field Tasks - Field communicators have existed for as long as intelligent devices. The early problem of plants having to grapple with many different communicators was solved already in the mid nineties by standard protocols like HART and Foundation fieldbus together with the Electronic Device Description Language (EDDL, formerly just known as DDL), an integral part of both technologies. A single universal field communicator supports all instruments, an arsenal of many communicators is no longer required. Use of Windows software from the central control room has since become possible thanks to multiplexers and digital communication interfaces embedded in control system I/O modules. These systems may access data in devices using HART, FOUNDATION fieldbus, PROFIBUS, WirelessHART, or a combination of two or more of these. Although many maintenance tasks can be done remotely from centrally located device management software part of Asset Management Solution (AMS), there are several other tasks that must still be carried out in the field right next to the device. Because of such field work, a compact field communicator is highly valued by maintenance technicians. A notebook computer is not ideal. EDDL is the only technology suitable for portable communicators because it works on embedded operating system used in such devices. IEC 61804-3 graphical enhancements the EDDL now make field communicators easier to use and powerful enough for complex devices.
Calibration Trim Wizard using EDDL - Narrated by Emerson's Harish Jayaraman this video shows how calibration trim is simplified by wizards from software or handheld communicator from different vendors using EDDL - from YouTube.

Other General Test and Calibration Links

Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results - Barry N. Taylor and Chris E. Kuyatt - This is NIST Technical Note 1297 as it was published.

U. S. Army Corps of Engineers Process Instrument And Control Checklist - This is a very useful checklist which is designed to facilitate the performance evaluation of process instrumentation and control systems used to operate and monitor treatment processes and equipment.

On Site Flow Calibration is Painful but Necessary - by David W. Spitzer - thanks to ControlGlobal.com. Some new product introductions have raised doubt about what in-situ calibration for flowmeters is, and whether it can be duplicated with simulators and calibrators with expanded diagnostics.

Calibrating and Testing Control Components on your Heat Process - What, When and How Should I Calibrate? - Arthur Holland, Holland Technical Skills - an excellent explanation on the basics of calibration - from dcnz.

Calibrating Non Destructive Testing Instruments - NDT Resource Centre-Calibration refers to the act of evaluating and adjusting the precision and accuracy of measurement equipment. In ultrasonic testing, several forms of calibration must occur. First, the electronics of the equipment must be calibrated to ensure that they are performing as designed. This operation is usually performed by the equipment manufacturer and will not be discussed further in this material. It is also usually necessary for the operator to perform a "user calibration" of the equipment. This user calibration is necessary because most ultrasonic equipment can be reconfigured for use in a large variety of applications.

A Guide to Low Resistance Measurement - You have to register to obtain this handbook which gives an overview of low resistance measurement techniques, explains common causes of errors and how to avoid them. We have also included useful tables of wire and cable characteristics, temperature coefficients and various formulas to ensure you make the best possible choice when selecting your measuring instrument and measurement technique - from Cropico.

Guide To Low Resistance Testing - Understanding and Measuring Low Resistance to Ensure Electrical System Performance - The purpose of this booklet is to help the engineer, technician or operator to understand the rationale behind low resistance, how to make a low resistance, how to select the proper instrument for the testing application and how to interpret and use the results - from Megger and Tech Rentals.

Getting Down to Earth - A Practical Guide to Earth Resistance Testing - Earth resistance is measured in two ways for two important fields of use:

Determining effectiveness of “ground” grids and connections that are used with electrical systems to protect personnel and equipment.
Prospecting for good (low resistance) “ground” locations, or obtaining measured resistance values that can give specific information about what lies somedistance below the earth’s surface (such as depth to bed rock). It is not the intent of this manual to go too deeply into the theory and mathematics of the subject. As noted in the references at the end, there are many excellent books and papers that cover these. Rather, the information herein is in simple language for easy understanding by the user in industry - from Megger and Weschler Instruments

The Expression of Uncertainty and Confidence in Measurement - M3003 - The general requirements that testing and calibration laboratories have to meet if they wish to demonstrate that they operate to a quality system, are technically competent and are able to generate technically valid results are contained within ISO/IEC 17025:2005. This international standard forms the basis for international laboratory accreditation and in cases of differences in interpretation remains the authoritative document at all times. M3003 is not intended as a prescriptive document, and does not set out to introduce additional requirements to those in ISO/IEC 17025:2005 but to provide amplification and guidance on the current requirements within the international standard. This 82 page document is certainly comprehensive - from www.ukas.com.

The Internet Resource for the International Temperature Scale of 1990 - Temperature Scale and General Temperature information for metrologists, scientists, calibration engineers and those with an interest in the temperature scale and its realisation.

Calibration of Test Equipment for Maintenance Purposes - The responsibility of an Approved Maintenance Organisation (AMO) is to provide within its Maintenance Organisation Manual (Policy and Procedures Manual (or equivalent document) a list of all test equipment that must be calibrated and the process to track the calibration - from Civil Aviation Safety Authority. Please note this is an archival copy and is not available from the source. However the information contained in it is very useful. Should there be any issue with it being on this website please advise This email address is being protected from spambots. You need JavaScript enabled to view it. and we will remove it.

The Following Papers are from BEAMEX:

Automated Calibration Planning Lowers Costs - Calibration is an essential element of any instrumentation maintenance program. However, sometimes calibration operations can be long and time-consuming. By planning the process and adding the right tools, efficiency can be improved and costs lowered substantially.
Traceable and Efficient Calibrations in the Process Industry - Today’s modern process plants, production processes and quality systems, put new and tight requirements on the accuracy of process instruments and on process control. Quality systems, such as the ISO9000 and ISO14000 series of quality standards, call for systematic and well documented calibrations, with regard to accuracy, repeatability, uncertainty, confidence levels etc.
The Safest Way to Calibrate - An Introduction to Intrinsically Safe Calibrators - There are industrial environments where calibrations should not only be made accurately and efficiently, but also safely. When safety becomes a top priority issue in calibration, intrinsically safe calibrators enter into the picture.

The Following Papers are from Fluke:

Many Technical Calibration Papers including the following can be found thanks to Fluke, you have to register but it is worth it.
A Poor Man's Resistance Bridge
A Preliminary Assessment of the Effectiveness of 5700A Artifact Calibration
A Traceability Technique for Complex Waveform Generators
A Wheatstone Bridge for the Computer Age
An Application of the Guide to Measurement Uncertainty
An Assessment of Artifact Calibration Effectiveness for a Multifunction Calibrator
Calibration Data Management: Meeting the Reporting Requirements of ISO/IEC FDIS 17025 Future Developments in Oscilloscope Calibration
Maintenance and Calibration of HART Field Instrumentation
Why Calibrate Test Equipment? - You’re serious about your electrical test instruments. You buy top brands, and you expect them to be accurate. You know some people send their digital instruments to a metrology lab for calibration, and you wonder why. After all, these are all electronic - there’s no meter movement to go out of balance. What do those calibration folks do, anyhow - just change the battery? These are valid concerns, especially since you can’t use your instrument while it’s out for calibration. But, let’s consider some other valid concerns. For example, what if an event rendered your instrument less accurate, or maybe even unsafe? What if you are working with tight tolerances and accurate measurement is key to proper operation of expensive processes or safety systems? What if you are trending data for maintenance purposes, and two meters used for the same measurement significantly disagree?
Measurement Uncertainty - How does DMM Accuracy affect your next Measurement? - Measurement uncertainty is an estimate of the possible error in a measurement. It's also an estimate of the range of values which contain the true value of the measured quantity. It's also the probability that the true value lies within a stated range of values.

The following Calibration Links are from Dickson:

Are All Metrology Labs Alike? - Short answer - NO!!! - In fact, to those of us in the industry who truly know what it takes to recalibrate instruments to objectively defined standards, a better question might be - Are you using the equivalent of a meat thermometer to validate conditions in your processing plant or laboratories?
“Before” Calibrations Count More than Many Think - As most know, temperature and humidity dataloggers and chart recorders need to be recalibrated periodically to ensure this accuracy, and competent quality managers need to establish schedules for recalibrations that reflect due diligence to monitor hot temperatures and humidity are kept within acceptable and pre-defined tolerances. But "recalibration" can mean different things, and what could be termed "recalibration on the cheap" does NOT demonstrate the accuracy of your recorded data (instruments).
Monitoring Revisited - While most pharmaceutical quality managers realize the importance of temperature and humidity tracking to guarantee both quality and compliance, the way in which many go about it is adding hidden costs. Technology for temperature/humidity tracking continues to evolve, and there are numerous time-saving features in recent temperature/humidity data loggers that can make a difference. On one hand, some quality managers are doing too much to track temperature/humidity data, while on the other hand some are doing too little. For many, it’s timely to revisit temperature and humidity monitoring. Here are some key points to consider.
Monitoring Temperature and Humidity - Monitoring temperature and/or humidity conditions is an essential ingredient of a wide range of quality assurance applications. There are many common methodological errors, however, in ways that this task is approached that either compromise quality standards or add unnecessary time and expense to the monitoring task. Insufficient calibration of temperature and humidity monitoring instruments is high on the list of problematic areas. Mismatching technology to the monitoring task at hand is another problematic area. This article revisits technology trends in monitoring instrumentation, provide tips on calibration and discuss common methodological errors that quality managers should avoid.
Temperature Calibration Frequently Asked Questions - Asks the questions What is calibration?, Why should I calibrate?, Who says what is accurate? Recalibration: what and why?

Electrical Measurement Safety

Electrical Measurement Safety Program - Every day, an average of 9,000 U.S. workers suffer disabling injuries on the job. Anyone performing electrical measurements should understand the safety standards and be certain their tools meet code. This page from Fluke is an excellent Safety Resource.

Video - Electrical Measurement Safety - This hour long session provides an awareness of electrical measurement hazards; a better understanding of the safety specifications for digital multimeters and testers; an understanding of the four installation measurement categories and; how to minimize and avoid electrical measurement hazards- You will need to register to see this video - from Fluke.

10 Mistakes People Make Working on Electrical Systems - Jim White - This list gets you thinking. We go through life making small mistake after small mistake and nothing happens, until we happen to get the wrong alignment of small mistakes and have an accident. Once the accident starts, we have no control over it, so the best thing to do is to avoid the small mistakes and tighten up the way we work - from Shermco Industries and Fluke.

Test and Calibration Standards

Standards Related to Temperature and Calibration - A list of ASTM standards.

Temperature Instrument Calibration

The following temperature calibration links are compliments of ISOtech:

A Review of Some of the Best Articles Written about Water and its Triple Point - Details of articles on this subject.
Calibrating Thermometers - Dave Ayres and Anne Blundell - A thermometer without a traceable calibration route to recognised National Standards is fairly useless. Yet we all buy mass produced thermometers which are supplied without a calibration and use them. We all hope that the manufacturer has been conscientious and has at least carried out calibration checks on batch samples and has claimed a level of accuracy to the batch. But has the manufacturer used suitable standards for the calibration?
Improved Sterilizer Tests - Dave Ayres and Dave Hill - Scottish Healthcare Supplies Sterilizer Test Group assessed various established methods of on-site temperature calibration and realised there might be shortcomings in commercially available "complete" systems. The guidelines require tests on sterilizer systems to be carried out within a system uncertainty of ±0.5^°C but the assessment showed that in many cases "complete" systems could produce a system uncertainty of ±1.0^° or worse. (Temperature monitoring in sterilizer systems is critical ensuring that microbiological viability is eliminated from the product).
Industrial Measurements with very Short Immersion - J. P. Tavener, D. Southworth, D. Ayres, N. Davies - One major problem that keeps recurring is the request to calibrate, or in some other way to evaluate, very short industrial temperature sensor assemblies. These sensors are so short that the sensor does not attain the temperature of its surroundings. Two distinct methods are possible, in method one the assembly is immersed in a comparison bath sufficiently to eliminate the stem conduction effect, even if this method creates a different result than achieved in-situ. Method two attempts to simulate the application in practice and provide a similar stem conduction error as the assembly sees in practice.
Automating Temperature Calibration Baths with Simple Low Cost Image Acquisition - David J. Southworth - A low cost video camera, “Web Cam” is used in conjunction with a PC and Temperature Calibration Bath to automatically calibrate handheld digital thermometers which have no provision to be connected to an external computer.
Stem Conduction and Light Piping in ITS-90 Fixed Point Cell Assemblies At A UKAS Laboratory - J. P. Tavener & A. Blundell - Standard Platinum Resistance Thermometers (SPRTs) with length-below-handle of only 480mm are regularly submitted for calibration at ITS-90 fixed points from -200 ^°C to +660 ^°C. The length of the thermometer limits the maximum size of fixed point cell that can be used to calibrate the thermometers. Stem conduction effects have been measured at zinc and aluminium temperatures in resealable cells. These have been quantified and eliminated by adopting a cell design with a very small connection between cell and gas supply.
Temperature Calibration: Depths of Immersion - John P. Tavener - Of all the sources of errors and uncertainties in thermal calibration by far the largest source of error and least understood effect is that of immersion of unit under test, and the reference standard.
Primary Laboratory Comparisons - The most accurate measurements made in a Primary Temperature Laboratory are during intercomparisons of ITS-90 fixed point cells, and in particular inter-comparing water triple point cells. To assess the stability of the water triple point, a laboratory ideally needs to be able to measure differences of just one or two micro degrees. At the Northern Temperature Primary Laboratory (NTPL) we found the spread of results too large to give a satisfactory result. Consulting the literature, and in particular Tischler &Prado [3] we eventually developed a 3 current technique from which we were able to calculate the zero current resistance to within 1 or 2 micro degrees. This paper describes in detail our method.
Gold/Platinum Thermocouple and the DC Measurement Requirements - John P. Tavener - This is an interesting article highlighting why thermocouples should not be used for high accuracy applications. Thermocouples are nasty complicated ill understood things that measure temperature differences badly and should be avoided at all cost. Calibration of thermocouples - if possible at all - is a topic fraught with measurement problems. This author has avoided them as far as possible for the past 30 years and refuses to calibrate most types of thermocouple in Isotech’s UKAS Laboratory. A great friend of mine once said of a fellow scientist “what a pity that such a great man should have devoted so much of his life to such an inferior thing”. ITS-90 removed them in favour of the Standard Platinum Resistance Thermometer. The limiting factor with all normal thermocouples is that one or both of the thermo-elements is an alloy and an alloy can not be produced that is homogeneous. This means that, because the Emf of a thermocouple is generated along the wire where there exists a thermal gradient, if the thermal gradient is moved along the thermocouple the Emf will change. This limits the best thermocouple accuracy to about ±0.3^°C, 2 sigma. If both thermo-elements were of pure metal, then this limitation would not exist, giving the possibility of more accurate thermocouple measurement.

Recommended Book - Traceable Temperatures - An Introduction to Temperature Measurement and Calibration - J.V. Nicholas and D.R. White, John Wiley + Sons, 2nd Edition Download Chapter One: Measurement and Traceability Purchase from Amazon.co.uk.

Useful Books on Instrument Calibration and Measurement

Calibration: A Technician's Guide - This comprehensive review of calibration provides an excellent foundation for understanding principles and applications of the most frequently performed tasks of a technician. Topics addressed include terminology, bench vs. field calibration, loop vs. individual instrument calibration, instrument classification systems, documentation, and specific calibration techniques for temperature, pressure, level, flow, final control, and analytical instrumentation. The book is designed as a structured learning tool with questions and answers in each chapter. An extensive appendix containing sample P&IDs, loop diagrams, spec sheets, sample calibration procedures, and conversion and reference tables serves as a very useful reference. If you calibrate instruments or supervise someone that does, then you need this book.

Quality Calibration Handbook - Developing and Managing a Calibration Program - Quality calibration systems are the very foundation for improving research and development (R&D), production, and quality assurance arenas through accurate, reliable, and traceable calibrations of their test equipment. This book is about how to design, implement, maintain, and continuously improve a quality calibration system, with all the required documentation, traceability, and known uncertainty for each and every item of test equipment owned and used by any company, large or small. It will benefit companies that want to implement a program and also those that already have one in place. Calibration requirements vary across specific industries but every organization can use the quality calibration system described in this book as a foundation for its personalized program. By using the quality calibration system outlined and demonstrated, any organization can put together its own version to meet its specific requirements and/or regulations.

Loop Checking: A Technician's Guide - In today’s competitive markets, manufacturers strive to continually improve manufacturing performance to meet their business needs and goals. As process control loops have a major impact on a plant’s financial performance, focusing on loop performance is critical. This technician’s guide defines loop checking in the broader scope of control loop performance in addition to the more traditional terms of the plant startup. It discusses general methods and practices that can be applied across many processes/industries. Featured topics include: loop checking basics, factory acceptance testing, wiring and loop checks, performance benchmarking, and sustaining performance.

Troubleshooting: A Technician's Guide - Troubleshooting loops and systems is something all technicians must do, but that few truly master. This newly revised edition draws on the author’s long experience as an instrument and electrical engineer and his maintenance expertise to provide a detailed look at the skills and knowledge required for troubleshooting. Interspersed with a wealth of practical detail and real-world examples are Mostia’s no-nonsense discussions of what a good troubleshooter needs to know. He provides an in-depth discussion of the basic logical framework that underlies all troubleshooting as well as advanced troubleshooting techniques. He also explores the causes of failures and the techniques that engineers and technicians use to trace them down. This new edition covers troubleshooting methods, both basic and advanced, hints and troubleshooting aids, troubleshooting safety, basic maintenance concepts, information about training, and the developing troubleshooting skills. It also includes numerous examples of troubleshooting problems in mechanical systems, process connections, pneumatic systems, electrical systems, electronic systems, and valves. Mostia also explores test equipment, programmable electronic systems, communication circuits, transient problems, and software.

Start-Up: A Technician's Guide - When new plants or systems go online, the control systems technician (CST) faces special challenges. The author explores and explains the crucial role of a technician in this process. This book offers you a clear overview of typical start-up responsibilities. From the first team meeting to the last round of tuning and loop checking, Harris uses her extensive experience with process control plants to walk you through the issues and skills typically required. Each chapter includes self-study learning objectives, practice questions and exercises, answers, and listings of relevant standards. Written with the technician in mind, it is an application-oriented book that provides an overview of the scope of duties a technician must perform in real-world situations. Includes over 30 figures and tables: fully indexed.

Ultimate Calibration - 2nd Edition - This calibration handbook covering various topics about advanced calibration comprises 203 pages and 19 articles - Calibrators, calibration software and other related equipment have developed significantly during the past few decades in spite of the fact that calibration of measurement devices as such has existed for several thousands of years. Presently, the primary challenges of industrial metrology and calibration include how to simplify and streamline the entire calibration process, how to eliminate double work, how to reduce production down-time, and how to lower the risk of human errors. All of these challenges can be tackled by improving the level of system integration and automation. Calibration and calibrators can no longer be considered as isolated, stand-alone devices, systems or work processes within a company or production plant. Just like any other business function, calibration procedures need to be automated to a higher degree and integrated to achieve improvements in quality and efficiency. In this area, Beamex aims to be the benchmark in the industry. This book is the 2nd edition of Ultimate Calibration. The main changes to this edition include numerous new articles and a new grouping of the articles to make it easier to find related topics. The new topics covered in the edition mainly discuss paperless calibration, intelligent commissioning, temperature calibration and configuring, and calibration of smart instruments - from Beamix.